1-羟基-1-环已基甲酸乙酯合成路线 (共 15 条)
反应条件
sulfuric acid in benzene Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 359 - 366
反应条件
1: aq. HCl 2: p-TsOH View Scheme
参考文献
Chimia, , vol. 57, # 11 p. 697 - 701
反应条件
1: sodium metabisulphite / H2O / 2 h / 25 °C 2: conc. HCl / acetic acid / 3 h / Heating 3: 42 percent / conc. H2SO4 / benzene / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 359 - 366
反应条件
1: concentrated sulfuric acid 3: alcoholic hydrochloric acid View Scheme
参考文献
Chemische Berichte, , vol. 48, p. 1394
参考文献
Chemische Berichte, , vol. 48, p. 1394
反应条件
(i) LDA, THF, (ii) O2; Multistep reaction;
参考文献
Tetrahedron Letters, , p. 1731 - 1734
反应条件
phosphorus pentoxide Hydrierung des entstandenen Cyclohexen-(1)-carbonsaeure-(1)-aethylesters mit Wasserstoff und Nickel bei 130-180grad;
参考文献
Darzens
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1907 , vol. 144, p. 329
参考文献
v. Auwers; Krollpfeiffer
Chemische Berichte, 1915 , vol. 48, p. 1394
参考文献
v. Auwers; Krollpfeiffer
Chemische Berichte, 1915 , vol. 48, p. 1394
反应条件
lithium aluminium tetrahydride in diethyl ether 1.) 30 min, 2.) reflux, 1 h;
参考文献
Carr, Graham; Whittaker, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 359 - 366