N,N-二甲基-2-苯乙胺合成路线 （共 89 条）
反应条件
potassium permanganate; N-benzyl-N,N,N-trimethyl-ammonium chloride in dichloromethane
3 h; Heating; Yield given. Yields of byproduct given;
参考文献
Markgraf, J. Hodge; Sangani, Poorab K.; Finkelstein, Manuel
Synthetic Communications, 1997 , vol. 27, # 7 p. 1285 - 1290
反应条件
potassium tert-butylate; tert.-butyl lithium in tetrahydrofuran; pentane
T=-78 - -60°C; 1 h; Inert atmosphereSchlenk technique;
参考文献
Unkelbach, Christian; Rosenbaum, Hannah S.; Strohmann, Carsten
Chemical Communications (Cambridge, United Kingdom), 2012 , vol. 48, # 86 p. 10612 - 10614,3
Title/Abstract Show Details
Unkelbach, Christian; Rosenbaum, Hannah S.; Strohmann, Carsten
Chemical Communications, 2012 , vol. 48, # 86 p. 10612 - 10614
反应条件
potassium permanganate; N-benzyl-N,N,N-trimethyl-ammonium chloride in dichloromethane
3 h; Heating; Yield given. Yields of byproduct given;
参考文献
Markgraf, J. Hodge; Sangani, Poorab K.; Finkelstein, Manuel
Synthetic Communications, 1997 , vol. 27, # 7 p. 1285 - 1290
参考文献
Kometani; Shiotani; Mitsuhashi
Chemical and Pharmaceutical Bulletin, 1976 , vol. 24, # 2 p. 342 - 349
参考文献
Riddell, Frank G.; Rogerson, Martin
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 2 p. 249 - 255
反应条件
1: 1.) ether, n-BuLi, 24 h 2.) 30 min
3: 1.) 5percent Pd/C / 1.) diphenyl ether, 270 deg C, 3 h 2.) ethyl alcohol, reflux
View Scheme
参考文献
Narasimhan, N. S.; Ranade, A. C.; Bhide, B. H.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 439 - 440
参考文献
Barger
Journal of the Chemical Society, 1909 , vol. 95, p. 2196
参考文献
Barger
Journal of the Chemical Society, 1909 , vol. 95, p. 2196
反应条件
(batho)2CuII (batho = 2,9-dimethyl-4,7-diphenyl-1,10-phenanthrolinedisulfonate); water in methanol
T=25°C; 24 h; pH 8; Rate constant;
参考文献
Wang, Fengjiang; Sayre, Lawrence M.
Journal of the American Chemical Society, 1992 , vol. 114, # 1 p. 248 - 255
