3,5-二甲基吡唑-1-硫代甲酰胺合成路线 (共 29 条)
反应条件
hydrogenchloride in water 6.5 h;
参考文献
New Journal of Chemistry, , vol. 29, # 6 p. 833 - 840
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 25, p. 1054 - 1055
反应条件
hydrogenchloride in methanol
参考文献
Mendeleev Communications, , vol. 17, # 6 p. 335 - 336
反应条件
in dimethylsulfoxide-d6 T=100°C; 0.5 h;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 26, # 9 p. 1051 - 1060
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 26, # 9 p. 1260 - 1270
反应条件
sodium carbonate in neat (no solvent, solid phase) T=20°C; Hantzsch Thiazole Synthesis; 0.0833333 h; Green chemistry;
参考文献
Aggarwal, Ranjana; Kumar, Sunil; Singh, Shiv P.
Journal of Sulfur Chemistry, 2012 , vol. 33, # 5 p. 521 - 525,5
反应条件
in ethanol 6 h; Heatingalso reaction with other phenacyl bromides; Product distribution;
参考文献
Singh, S. P.; Sehgal, Subhash; Singh, Lukhvinder; Dhawan, S. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 154 - 155
反应条件
in dimethylsulfoxide-d6 T=100°C; 3 h;
参考文献
Chawla, Sukhvinder K.; Kaur, Simrat; Gupta, Nidhi; Hundal, Geeta
Mendeleev Communications, 2007 , vol. 17, # 6 p. 335 - 336
反应条件
in ethanol 2.5 h; Heating; Yield given;
参考文献
Mamedov, V. A.; Litvinov, I. A.; Efremov, Yu. Ya.; Valeeva, V. N.; Rizvanov, I. Kh.; et al.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 5.2 p. 860 - 866
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 5 p. 1042 - 1050
参考文献
Scott et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 820,822
参考文献
Scott et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 820,822