3,5-二甲-2-乙吡啶合成路线 (共 24 条)
反应条件
potassium permanganate T=20°C;
参考文献
Duerkopf; Goettsch
Chemische Berichte, 1890 , vol. 23, p. 687,1111
反应条件
potassium permanganate
参考文献
Duerkopf; Goettsch
Chemische Berichte, 1890 , vol. 23, p. 691
Full Text Show Details
Duerkopf; Schlaugk
Chemische Berichte, 1888 , vol. 21, p. 835,2707
反应条件
1: 2,3,5-trimethyl-pyridine With n-butyllithium in diethyl ether; hexane
1.16667 h; Inert atmosphere;
2: methyl iodide in diethyl ether; hexane
T=-78 - 20°C; Inert atmosphere;
参考文献
Verdia, Pedro; Gonzalez, Emilio J.; Rodriguez-Cabo, Borja; Tojo, Emilia
Green Chemistry, 2011 , vol. 13, # 10 p. 2768 - 2776
反应条件
tetrahydropyridine hydrochloride in toluene
T=200°C; 2 h; autoclave;
参考文献
Vijn; Arts; Green; Castelijns
Synthesis, 1994 , # 6 p. 573 - 578
反应条件
carbonylchloro[4,5-bis(diisopropylphosphinomethyl)acridine]hydridoruthenium(II); water in 1,4-dioxane
T=120°C; 18 h; Schlenk techniqueInert atmosphere;
参考文献
Khusnutdinova, Julia R.; Ben-David, Yehoshoa; Milstein, David
Angewandte Chemie - International Edition, 2013 , vol. 52, # 24 p. 6269 - 6272
Angew. Chem., 2013 , vol. 125, # 24 p. 6389 - 6392,4
反应条件
ammonia; hydrogen; LaCaY; rhodium
T=210°C; P=97507.8 Torr; 5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Kosolapova, B. S.; Levin, D. Z.; Sominskii, S. D.; Rar, L. F.; Mortikov, E. S.; Lapidus, A. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 11 p. 2244 - 2248
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 11 p. 2481 - 2486
反应条件
palladium dichloride
T=170°C; 6 h; Autoclave;
参考文献
Atnabaeva; Muslimov; Khusnutdinov; Dzhemilev
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 12 p. 1831 - 1835
反应条件
ammonia
T=150°C; im Rohr;
参考文献
Waage
Monatshefte fuer Chemie, 1883 , vol. 4, p. 725
参考文献
Ploechl
Chemische Berichte, 1887 , vol. 20, p. 722
反应条件
palladium dichloride
T=160°C; 6 h; Autoclave;
参考文献
Atnabaeva; Muslimov; Khusnutdinov; Dzhemilev
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 12 p. 1831 - 1835