1,4-二甲基-2-碘苯合成路线 (共 37 条)
反应条件
Cu-Hg
T=200 - 260°C;
参考文献
Kovyrzina,K.A.; Tsvetkova,T.A.
Journal of Organic Chemistry USSR (English Translation), 1974 , vol. 10, p. 1078 - 1080
Zhurnal Organicheskoi Khimii, 1974 , vol. 10, # 5 p. 1067 - 1070
反应条件
Cu-Hg
T=220 - 260°C;
参考文献
Kovyrzina,K.A.; Tsvetcova,T.A.
Journal of Organic Chemistry USSR (English Translation), 1977 , vol. 13, p. 2227 - 2229
Zhurnal Organicheskoi Khimii, 1977 , vol. 13, # 11 p. 2395 - 2398
反应条件
N-bromosuccinmide; 1,1'-azobis (cyclohexanecarbonitrile) in 1,2-dichloro-ethane
Heatingirradiation;
参考文献
Vaidyanathan, Ganesan; Shankar, Sriram; Affleck, Donna J.; Alston, Kevin; Norman, Joseph; Welsh, Philip; LeGrand, Holly; Zalutsky, Michael R.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 7 p. 1649 - 1656
反应条件
sulfur dioxide; nitric acid; acetic anhydride
参考文献
Varma; Raman
Journal of the Indian Chemical Society, 1935 , vol. 12, p. 540
反应条件
Merrifield resin-bound dicyclohexylphosphinobiphenyl ligand; sodium t-butanolate; palladium diacetate in toluene
T=80°C;
参考文献
Parrish; Buchwald
Journal of Organic Chemistry, 2001 , vol. 66, # 11 p. 3820 - 3827
反应条件
copper(l) iodide; triphenylphosphine; palladium dichloride in diethylamine
T=54 - 56°C;
参考文献
Rudenko, A. P.; Vasil'ev, A. V.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 10 p. 1360 - 1379
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 10 p. 1502 - 1522
反应条件
[(PPh3)3Pd] in tetrahydrofuran
T=22°C; 48 h; other reagent, reaction time; Product distribution;
参考文献
Negishi, Ei-ichi; Kotora, Martin; Xu, Caiding
Journal of Organic Chemistry, 1997 , vol. 62, # 25 p. 8957 - 8960