(NZ)-N-(2-甲基环己亚基)羟胺合成路线 (共 16 条)
反应条件
hydroxylamine hydrochloride; sodium acetate in ethanol; water 1.) steam bath, 1-5 h, 2.) room temp.;
参考文献
Hutchins, Robert O.; Su, Wei-Yang; Sivakumar, Ramachandran; Cistone, Frank; Stercho, Yuriy P.
Journal of Organic Chemistry, 1983 , vol. 48, # 20 p. 3412 - 3422
反应条件
n-butyllithium; hexamethyl-silane in tetrahydrofuran; hexane 24 h; Ambient temperature;
参考文献
Hwu, Jih Ru; Tseng, Wen Nan; Patel, Himatkumar V.; Wong, Fong Fuh; Horng, Den-Nan; Liaw, Ben Ruey; Lung Ching, Lin
Journal of Organic Chemistry, 1999 , vol. 64, # 7 p. 2211 - 2218
反应条件
(i) NOCl, (ii) NaBH4; Multistep reaction;
参考文献
Biela,R. et al.
Journal fuer Praktische Chemie (Leipzig), 1966 , vol. 33, p. 282 - 292
反应条件
hydrogen; palladium on activated charcoal in methanol
参考文献
Biela,R. et al.
Journal fuer Praktische Chemie (Leipzig), 1966 , vol. 33, p. 282 - 292
反应条件
sodium tungstate; dihydrogen peroxide in methanol
参考文献
Kahr,K.; Berther,C.
Chemische Berichte, 1960 , vol. 93, p. 132 - 136
反应条件
sodium hydroxide; hydroxylamine hydrochloride liquid form;
参考文献
v. Auwers; Bahr; Frese
Justus Liebigs Annalen der Chemie, 1925 , vol. 441, p. 67
反应条件
sodium hydroxide; ethanol
参考文献
Taguchi,T. et al.
Chemical and Pharmaceutical Bulletin, 1963 , vol. 11, # 2 p. 222 - 225
反应条件
nitrosyl chloride Irradiation;
参考文献
Deschamps,A. et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1965 , vol. 260, p. 4514 - 4517
反应条件
indium trifluoromethanesulfonate in acetonitrile Beckmann rearrangement; 3.5 h; Heating;
参考文献
Barman, Dhiren C.; Gohain, Mukut; Prajapati, Dipak; Sandhu, Jagir S.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 1 p. 154 - 156
反应条件
sulfuric acid T=120°C; Title compound not separated from byproducts;
参考文献
Hermecz, Istvan; Vasvari-Debreczy, Lelle; Horvath, Agnes; Balogh, Maria; Koekoesi, Jozsef; et al.
Journal of Medicinal Chemistry, 1987 , vol. 30, # 9 p. 1543 - 1549