N-甲酰基-2-甲氧基-2-甲基-丙胺合成路线 (共 6 条)
参考文献
E. R. Squibb and Sons, Inc.
Patent: US4864051 A1, 1989 ;
反应条件
formic acid; acetic anhydride
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4988827 A1, 1991 ;
反应条件
triethylamine 68 h; Heating / reflux;
参考文献
DRAXIS Specialty Pharmaceuticals Inc.
Patent: US2008/102028 A1, 2008 ;
Location in patent: Page/Page column 9; 11 ;
反应条件
triethylamine; trichlorophosphate in dichloromethane T=-5 - 3°C; Product distribution / selectivity;
参考文献
DRAXIS Specialty Pharmaceuticals Inc.
Patent: US2008/102028 A1, 2008 ;
Location in patent: Page/Page column 9; 11-12 ;
反应条件
formamide; triethylamine in dichloromethane; water
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4988827 A1, 1991 ;
反应条件
sodium hydrogencarbonate; triethylamine in dichloromethane; water
参考文献
E. R. Squibb and Sons, Inc.
Patent: US4864051 A1, 1989 ;