5-羟基甲基-5-甲基-1,3-二氧己烷合成路线 （共 4 条）
反应条件
2-chloro-1,3,2-dithioborolane in dichloromethane T=-78°C; 0.75 h;
参考文献
Williams, D.R.; Sakdarat, Santi
Tetrahedron Letters, 1983 , vol. 24, # 37 p. 3965 - 3968
反应条件
toluene-4-sulfonic acid; lithium bromide in dichloromethane T=23°C; 0.75 h;
参考文献
Gras, Jean-Louis; Nouguier, Robert; Mchich, Mohammed
Tetrahedron Letters, 1987 , vol. 28, # 52 p. 6601 - 6604
反应条件
toluene-4-sulfonic acid in toluene 3.5 h; Reflux;
参考文献
Oparina; Vysotskaya; Parshina; Khil'ko; Gusarova
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 10 p. 1434 - 1437
反应条件
1.1: Na / xylene / 2 h / Heating
1.2: 110 g / 15-crown-5 / xylene; dioxane
2.1: aq. H2SO4 / 10 h / Heating
3.1: 41 g / EtOH / Heating
View Scheme
参考文献
Bubnov, Alexej; Kaspar, Miroslav; Hamplova, Vera; Dawin, Ute; Giesselmann, Frank
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 425 - 436
