(Z)-十八碳-9-烯腈合成路线 （共 24 条）
反应条件
Grubb's 2nd generation catalyst in toluene T=80°C; P=760.051 Torr; 6 h;
参考文献
Arkema France
Patent: US2011/300590 A1, 2011 ;
Location in patent: Page/Page column 7 ;
反应条件
Grubb's 2nd generation catalyst T=60°C; P=760.051 Torr;
参考文献
Arkema France
Patent: US2011/224454 A1, 2011 ;
Location in patent: Page/Page column 8 ;
反应条件
dihydrogen peroxide; tungsten(VI) trioxide hydrate in water T=70°C; P=760.051 Torr; 6 h; ConcentrationTemperatureTime;
参考文献
US2013/345388 A1, ;
Paragraph 0151-0160 ;
反应条件
1.1: Grubb's 2nd generation catalyst / 60 °C / 760.05 Torr 2.1: ozone / hydrochloric ether / 0.08 h / -40 °C 2.2: 0.5 h / Reflux View Scheme
参考文献
Arkema France
Patent: US2011/224454 A1, 2011 ;
反应条件
ammonia; hydrogen; Ni-doped silica; 4-methylbenzoic acid amide T=140°C; P=26252.6 Torr; 3.5 h; Product distribution / selectivity;
参考文献
LION AKZO CO., LTD.
Patent: WO2007/29571 A1, 2007 ;
Location in patent: Page/Page column 10-12 ;
反应条件
T=150 - 175°C; unter Druck;
参考文献
du Pont de Nemours and Co.
Patent: US2230390 , 1939 ;
反应条件
sodium hydroxide in ethanol; water Heating;
参考文献
Tetrahedron Letters, , vol. 32, # 28 p. 3321 - 3324
反应条件
sodium azide; triethylamine; triphenylphosphine; [bis(2-methoxyethyl)amino]-sulfur trifluoride in dichloromethane; dimethyl sulfoxide
T=0 - 20°C; 0.5 h;
参考文献
Kangani, Cyrous O.; Day, Billy W.; Kelley, David E.
Tetrahedron Letters, 2007 , vol. 48, # 34 p. 5933 - 5937
