1: 1.) H2SO4, H2O2 (28percent w/v), 2.) NaOH / 1.) 40 deg C, 8 h, 2.) MeOH, water, reflux, 5 h 2: 52.5 g / 5percent methanolic HCl / 48 h / Ambient temperature View Scheme
参考文献
Thakur, S. B.; Jadhav, K. S.; Bhattacharyya, S. C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 675 - 683
triethylamine; trichlorophosphate in dichloromethane
参考文献
Vig, O. P.; Trehan, I. R.; Kad, G. L.; Dhawan, R. K.; Grewal, M. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 8 p. 688 - 691
Vig, O. P.; Trehan, I. R.; Kad, G. L.; Dhawan, R. K.; Grewal, M. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 8 p. 688 - 691
