反应条件
sodium methylate
1.) sodium methoxide, dioxane, diol, 10 min 2.) 1,2-bis<2'-(toluene-p-sulphonyloxy)ethoxy>ethane, dioxane, 5 min, reflux; Multistep reaction;
参考文献
Bowsher, Brian R.; Rest, Antony J.; Main, Brian G.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 1421 - 1426