1-(苯氧基甲基)-1H-苯并噻唑合成路线 （共 14 条）
反应条件
sodium hydroxide 1.) EtOH, r.t., 1 h, 2.) DMF, 65-70 deg C, 15 h;
参考文献
Katritzky, Alan R.; Serdyuk, Larisa; Xie, Linghong
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 6 p. 1059 - 1064
反应条件
in methanol; toluene 2 h; Heating;
参考文献
Katritzky, Alan R.; Rachwal, Stanislaw; Rachwal, Bogumila
Journal of Organic Chemistry, 1989 , vol. 54, # 26 p. 6022 - 6029
反应条件
1: toluene / 0.75 h / Heating 2: SOCl2 / toluene / 2 h / Heating 3: 87 percent / toluene; methanol / 2 h / Heating View Scheme
参考文献
Dumas, Aaron M.; Bode, Jeffrey W.
Organic Letters, 2012 , vol. 14, # 8 p. 2138 - 2141
反应条件
1: SOCl2 / toluene / 2 h / Heating 2: 87 percent / toluene; methanol / 2 h / Heating View Scheme
参考文献
Dumas, Aaron M.; Bode, Jeffrey W.
Organic Letters, 2012 , vol. 14, # 8 p. 2138 - 2141
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-78 - 20°C; 1.08333 h; 2: With acetic acid T=80°C; 0.5 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 78, # 3 p. 477 - 486
反应条件
Yield given. Multistep reaction;
参考文献
Katritzky, Alan R.; Lang, Hengyuan; Wang, Zuoquan; Lie, Zhu
Journal of Organic Chemistry, 1996 , vol. 61, p. 7551 - 7557
反应条件
1: 95 percent / n-BuLi / tetrahydrofuran; hexane / 12 h / -78 - 20 °C 2: 68 percent / benzene / 12 h / Heating 3: 74 percent / diethyl ether / 1) -78 deg C, 0.5 h; 2) rt, 48 h View Scheme
参考文献
Katritzky, Alan R.; Wang, Jin; Karodia, Nazira; Li, Jianqing
Journal of Organic Chemistry, 1997 , vol. 62, # 12 p. 4142 - 4147
反应条件
n-butyllithium; toluene-4-sulfonic acid Multistep reaction; var. aldehydes; proposed mechanism; Product distribution;
参考文献
Katritzky, Alan R.; Yang, Zhijun; Moutou, Jean-Luc
Tetrahedron Letters, 1995 , vol. 36, # 6 p. 841 - 844
反应条件
n-butyllithium; sulfuric acid Yield given. Multistep reaction;
参考文献
Katritzky, Alan R.; Lang, Hengyuan; Wang, Zuoquan; Lie, Zhu
Journal of Organic Chemistry, 1996 , vol. 61, p. 7551 - 7557
反应条件
in diethyl ether; benzene Heating;
参考文献
Katritzky, Alan R.; Rachwal, Stanislaw; Rachwal, Bogumila
Journal of Organic Chemistry, 1989 , vol. 54, # 26 p. 6022 - 6029
