in neat (no solvent) byproducts: NH3; heating (70-85°C, then 110-120°C, several h); distn. (vac.);
参考文献
Voronkov, M. G.; Mirskov, R. G.; Chernova, V. G.; Ivanova, N. P.
Journal of General Chemistry USSR (English Translation), 1981 , vol. 51, p. 1430 - 1430
Zhurnal Obshchei Khimii, 1981 , vol. 51, p. 1678 - 1678
in further solvent(s) byproducts: MeCOOH; mixt. of trimethylacetoxysilane and finely ground boric acid heated at 110°C for 1 h; residue distilled in vac.; elem. anal.;
参考文献
Voronkov; Basenko; Mirskov; Adamovich
Russian Journal of Applied Chemistry, 2006 , vol. 79, # 10 p. 1721 - 1722
in neat (no solvent) Me3SiCl, Me3SiOSiMe3 and 2-propanol stirred for 30 min, boric acid added and stirred for 3 h; soln. filtered and concd., mixt. analysed by using combined gas chromatograph-mass spectroscopy;
CaH2 in neat (no solvent) byproducts: H2; react. under N2, slow addn. of the alcohol via syringe to B(OH)3 (ratio 3:1) and CaH2, cooling in a water bath, slow heating to 80-90°C for 12 h after abating the H2 gas evolution; distn. of the volatile products under reduced pressure (distn. pot temp. <= 120°C);
参考文献
Cole, T. E.; Quintanilla, R.; Rodewald, S.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1990 , vol. 20, p. 55 - 64
H(+) in water Kinetics; in acidic soln.; byproducts: decomposition products of 4-methyl-nioxime (H24MNx);
参考文献
Voloshin, Ya. Z.; Nazarenko, A. Yu.; Pol'shin, E. V.; Tyukhtenko, S. I.; Kostromina, N. A.
Theoretical and Experimental Chemistry, 1989 , vol. 25, p. 298 - 303
Teoreticheskaya i Eksperimental'naya Khimiya, 1989 , vol. 25, p. 322 - 328
