N,N'-二甲基乙二胺合成路线 （共 190 条）
反应条件
triethylamine in diethyl ether
15 h; Ambient temperature;
参考文献
Becker, W.; Schiebel, H. M.; Schmutzler, R.
Chemische Berichte, 1992 , vol. 125, # 4 p. 793 - 800
反应条件
triethylamine in chloroform
2 h; Ambient temperature;
参考文献
Regen, Steven L.; Mehrotra, Ashok; Singh, Alok
Journal of Organic Chemistry, 1981 , vol. 46, # 10 p. 2182 - 2184
参考文献
Bauer
Journal of the American Chemical Society, 1956 , vol. 78, p. 1945
反应条件
triethylamine; phosphorus trichoride in dichloromethane
1.) -40 --> -30 deg C, 2.) ambient temperature, 2 h;
参考文献
Anson; McGuigan
Journal of the Chemical Society - Series Chemical Communications, 1987 , vol. No. 17, p. 1275 - 1276
反应条件
triethylamine; trichlorophosphate in benzene
T=20°C; 2 h;
参考文献
Nunez, Andres; Berroteran, Dyanna; Nunez, Oswaldo
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 13 p. 2283 - 2289
参考文献
Hanessian, Stephen; Bennani, Youssef L.; Leblanc, Yves
Heterocycles, 1993 , vol. 35, # 2 p. 1411 - 1424
参考文献
Crouse, Heather F.; Potoma, Julianne; Nejrabi, Farhat; Snyder, Deanna L.; Chohan, Balwant S.; Basu, Swarna
Dalton Transactions, 2012 , vol. 41, # 9 p. 2720 - 2731
反应条件
in tetrahydrofuran
Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Xu, Daqiang; Prasad, Kapa; Repic, Oljan; Blacklock, Thomas J.
Tetrahedron Letters, 1995 , vol. 36, # 41 p. 7357 - 7360
反应条件
n-butyllithium
1.) -40 deg C, hexane, ether, 0.25h; 2.) -78 deg C, 12h, ether, hexane; Yield given. Multistep reaction;
参考文献
Gupta,K.D.; Shreeve,J.M.
Journal of Fluorine Chemistry, 1987 , vol. 34, p. 453
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.2, page 1 - 48
