反式1.4-二氯-2-丁烯合成路线 (共 76 条)
反应条件
sodium hypochlorite; oxygen; catamine AB T=40°C; 3 h;
参考文献
Grigoryan, G. S.; Karoyan, I. L.; Malkhasyan, A. Ts.; Martirosyan, G. T.; Artamkina, G. A.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1987 , p. 1039 - 1042
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 6 p. 1149 - 1153
反应条件
potassium carbonate in dimethyl sulfoxide 48 h;
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 1 p. 421 - 429
参考文献
Muskat; Northrup
Journal of the American Chemical Society, 1930 , vol. 52, p. 4054
参考文献
Lewina et al.
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 63,64
Chem.Abstr., 1949 , p. 6152
反应条件
copper(I) thiophene-2-carboxylate in diethyl ether; dichloromethane
T=-78°C; 4 h; Title compound not separated from byproducts.;
参考文献
Falciola, Caroline A.; Alexakis, Alexandre
Angewandte Chemie - International Edition, 2007 , vol. 46, # 15 p. 2619 - 2622
反应条件
sodium methylate in methanol
1.) RT, 45 min; 2.) 50 deg C, 3 h;
参考文献
Fujisawa, Tamotsu; Umezu, Kazuto; Kawashima, Masatoshi
Chemistry Letters, 1984 , p. 1795 - 1798
反应条件
4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran
T=0°C; 0.75 h;
参考文献
Guijarro, Albert; Yus, Miguel
Tetrahedron, 1994 , vol. 50, # 26 p. 7857 - 7864
反应条件
sodium ethanolate in ethanol
参考文献
Hosomi; Mikami; Sakurai
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 9 p. 2784 - 2794
反应条件
potassium carbonate in acetone
Heating;
参考文献
KANSAS STATE UNIVERSITY RESEARCH FOUNDATION
Patent: US2008/39528 A1, 2008 ;
反应条件
(i) NaOMe, MeOH, (ii) /BRN= 1719693/; Multistep reaction;
参考文献
Caserio, Marjorie C.; Fisher, Cindy L.; Kim, Jhong K.
Journal of Organic Chemistry, 1985 , vol. 50, # 22 p. 4390 - 4393