3-[[叔丁基二甲基硅烷基]氧基]-戊烷二酸 1-甲基酯合成路线 （共 8 条）
反应条件
potassium carbonate in tetrahydrofuran; methanol; water 1 h; Ambient temperature;
参考文献
Helvetica Chimica Acta, , vol. 70, p. 142 - 152
参考文献
Journal of Organic Chemistry, , vol. 49, # 19 p. 3657 - 3659
反应条件
1: 95 percent / imidazole / CH2Cl2 / 18 h / Ambient temperature 2: 1) NaOH 2) Ac2O / 1) MeOH, r.t. 2) benzene, 1.5h, reflux (better yield by using the di-K-salt of cpd.12 on a small scale basis) 3: Na / 1 h / 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 49, # 19 p. 3657 - 3659
反应条件
1: 95 percent / imidazole / CH2Cl2 / 18 h / Ambient temperature 2: 1) NaOH 2) Ac2O / 1) MeOH, r.t. 2) benzene, 1.5h, reflux (better yield by using the di-K-salt of cpd.12 on a small scale basis) 3: Na / 1 h / 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 49, # 19 p. 3657 - 3659
反应条件
methanol; C42H47F6N5O3 T=20°C;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 17 p. 3918 - 3922
反应条件
1: 19.4 g / imidazole / dimethylformamide / 12 h / Ambient temperature 2: 84 percent / K2CO3 / methanol; tetrahydrofuran; H2O / 1 h / Ambient temperature View Scheme
参考文献
Helvetica Chimica Acta, , vol. 70, p. 142 - 152
反应条件
1: 1) NaOH 2) Ac2O / 1) MeOH, r.t. 2) benzene, 1.5h, reflux (better yield by using the di-K-salt of cpd.12 on a small scale basis) 2: Na / 1 h / 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 49, # 19 p. 3657 - 3659
参考文献
Journal of Organic Chemistry, , vol. 63, # 9 p. 3037 - 3040
