反应条件
1: With [Ir(acetylacetonate)(1,5-cyclooctadiene)]; triphenylphosphine in N-methylpyrrolidone T=20 - 100°C; P=5250.53 Torr; Inert atmosphereAutoclave; 2: With hydrogen in N-methylpyrrolidone T=100°C; P=9750.98 Torr; 20 h; Autoclave; chemoselective reaction;
参考文献
Evonik Oxeno GmbH; Franke, Robert; Beller, Matthias; Jackstell, Ralf; Jennerjahn, Reiko; Piras, Irene
Patent: US2014/24860 A1, 2014 ;
Location in patent: Paragraph 0089 ;