反应条件
in neat (no solvent)
byproducts: water, ammonia; mixt. (molar ratio Sn-compd.:allylthiourea=2:1) heating up to 250°C in 1 h (gradual evacuation from 50 to 1.33 hPa); distn. of Bu3SnNCS after no water and ammonia came off; (Bu3Sn)2S isolation from residue;
参考文献
Gordetsov, A. S.; Latyaeva, V. N.; Bogdarin, Yu. A.; Boyarinov, G. A.; Dergunov, Yu. I.
Journal of General Chemistry USSR (English Translation), 1982 , vol. 52, p. 770 - 774
Zhurnal Obshchei Khimii, 1982 , vol. 52, p. 885 - 890