反应条件
in benzene react. under vac.; combination of Ph2GaCl and As-compd. in C6H6 (ratio Ph2GaCl : As-compd. = 3:1) in a bulb (cooled to -196°C, degassed), stirring for 16 days at 80°C; removal of solvent and Me3SiCl in vac., extn. with hot ligroin, addn. of C7H8 to the hot ext., cooling to -17°C for 3 days;
参考文献
Holley, William K.; Wells, Richard L.; Shafieezad, Soheila; McPhail, Andrew T.; Pitt, Colin G.
Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. 15 - 27
