反应条件
1: (E)-4-(4-hydroxy-3-methoxy-phenyl)-but-3-en-2-one With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.5 h; Inert atmosphere;
2: With lithium diisopropyl amide in tetrahydrofuran; hexane
T=-78°C; 3 h; Inert atmosphere;
3: hexanal in tetrahydrofuran; hexane
T=-78 - 0°C; Aldol Condensation; 4 h; Inert atmosphere;
参考文献
Lu, Dong-Liang; Li, Xiu-Zhuang; Dai, Fang; Kang, Yan-Fei; Li, Yan; Ma, Meng-Meng; Ren, Xiao-Rong; Du, Gao-Wei; Jin, Xiao-Ling; Zhou, Bo
Food Chemistry, 2014 , vol. 165, p. 191 - 197
