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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯酚
合成路线
（共 7752 条）
131002-10-3
6-甲基-1(2H)-异喹啉酮
+
108-95-2
苯酚
→
反应条件
209286-73-7
1-氯-6-甲基异喹啉
反应条件
potassium hydroxide in dichloromethane
参考文献
Aventis Pharma Deutschland GmbH
Patent: US6281227 B1, 2001 ;
108-95-2
苯酚
→
反应条件
24388-23-6
苯硼酸频哪醇酯
反应条件
1: 98 percent / pyridine / CH2Cl2 / 0.25 h / 0 °C 2: 86 percent / Et3N / PdCl2(dppf) / dioxane / Heating View Scheme
参考文献
Thompson, Alicia L. S.; Kabalka, George W.; Akula, Murthy R.; Huffman, John W.
Synthesis, 2005 , # 4 art. no. M05304SS, p. 547 - 550
100-20-9
对苯二甲酰氯
+
108-95-2
苯酚
→
反应条件
1539-04-4
对苯二甲酸二苯酯
反应条件
sodium hydroxide in diethyl ether; water T=0°C; 0.5 h;
参考文献
Chan, W.-C.; Mooney, J. A.; Windle, A. H.
Molecular Crystals and Liquid Crystals (1969-1991), 1989 , vol. 174, p. 75 - 88
589-87-7
对溴碘苯
+
13939-06-5
六羰基钼
+
108-95-2
苯酚
→
反应条件
1539-04-4
对苯二甲酸二苯酯
+
5798-76-5
反应条件
tributyl-amine in diethylene glycol dimethyl ether T=150°C; 12 h; Inert atmosphere; chemoselective reaction;
参考文献
Synthesis, , # 14 art. no. F31611SS, p. 2303 - 2309
108-95-2
苯酚
→
反应条件
1539-04-4
对苯二甲酸二苯酯
反应条件
1.1: acetic anhydride / 1 h / 60 °C / Inert atmosphere 1.2: 2.5 h / Inert atmosphere 2.1: palladium diacetate; triethylamine; [(t-Bu)3PH]BF4 / acetonitrile / 80 °C / Inert atmosphere View Scheme
参考文献
Ueda, Tsuyoshi; Konishi, Hideyuki; Manabe, Kei
Organic Letters, 2012 , vol. 14, # 12 p. 3100 - 3103
108-24-7
乙酸酐
+
95-48-7
邻甲酚
+
108-95-2
苯酚
→
反应条件
862742-99-2
+
1927-95-3
4-溴苯基乙酸酯
+
1829-37-4
1-乙酰氧基-2-溴苯
+
52727-92-1
反应条件
1: ortho-cresol; phenol With vanadate(V)-dependent bromoperoxidase I from Ascophyllum nodosum; dihydrogen peroxide; sodium bromide in water; tert-butyl alcohol T=25°C; 24 h; Enzymatic reaction; 2: acetic anhydride With Zn(ClO4)2*6H2O in diethyl ether T=23°C; 16 h; ConcentrationReagent/catalyst;
参考文献
Wischang, Diana; Hartung, Jens
Tetrahedron, 2012 , vol. 68, # 46 p. 9456 - 9463
88-18-6
邻叔丁基苯酚
+
108-24-7
乙酸酐
+
108-95-2
苯酚
→
反应条件
1927-95-3
4-溴苯基乙酸酯
+
1829-37-4
1-乙酰氧基-2-溴苯
+
1403457-44-2
反应条件
1: 2-tert-butylphenol; phenol With vanadate(V)-dependent bromoperoxidase I from Ascophyllum nodosum; dihydrogen peroxide; sodium bromide in water; tert-butyl alcohol T=25°C; 24 h; Enzymatic reaction; 2: acetic anhydride With Zn(ClO4)2*6H2O in diethyl ether T=23°C; 16 h; Concentration;
参考文献
Wischang, Diana; Hartung, Jens
Tetrahedron, 2012 , vol. 68, # 46 p. 9456 - 9463
108-24-7
乙酸酐
+
90-05-1
愈创木酚
+
108-95-2
苯酚
→
反应条件
1927-95-3
4-溴苯基乙酸酯
+
1829-37-4
1-乙酰氧基-2-溴苯
+
54145-18-5
+
244771-01-5
反应条件
1: 2-methoxy-phenol; phenol With vanadate(V)-dependent bromoperoxidase I from Ascophyllum nodosum; dihydrogen peroxide; sodium bromide in water; tert-butyl alcohol T=25°C; 24 h; Enzymatic reaction; 2: acetic anhydride With Zn(ClO4)2*6H2O in diethyl ether T=23°C; 16 h; ConcentrationReagent/catalyst;
参考文献
Wischang, Diana; Hartung, Jens
Tetrahedron, 2012 , vol. 68, # 46 p. 9456 - 9463
95-57-8
邻氯苯酚
+
108-24-7
乙酸酐
+
108-95-2
苯酚
→
反应条件
102932-05-8
4-溴-2-氯乙酸苯酯
+
1927-95-3
4-溴苯基乙酸酯
+
1829-37-4
1-乙酰氧基-2-溴苯
+
102932-04-7
反应条件
1: 2-chlorophenol; phenol With vanadate(V)-dependent bromoperoxidase I from Ascophyllum nodosum; dihydrogen peroxide; sodium bromide in water; tert-butyl alcohol T=25°C; 24 h; Enzymatic reaction; 2: acetic anhydride With Zn(ClO4)2*6H2O in diethyl ether T=23°C; 16 h; ConcentrationReagent/catalyst;
参考文献
Wischang, Diana; Hartung, Jens
Tetrahedron, 2012 , vol. 68, # 46 p. 9456 - 9463
367-12-4
2-氟苯酚
+
108-24-7
乙酸酐
+
108-95-2
苯酚
→
反应条件
1927-95-3
4-溴苯基乙酸酯
+
1829-37-4
1-乙酰氧基-2-溴苯
+
161424-78-8
反应条件
1: 2-Fluorophenol; phenol With vanadate(V)-dependent bromoperoxidase I from Ascophyllum nodosum; dihydrogen peroxide; sodium bromide in water; tert-butyl alcohol T=25°C; 24 h; Enzymatic reaction; 2: acetic anhydride With Zn(ClO4)2*6H2O in diethyl ether T=23°C; 16 h; ConcentrationReagent/catalyst;
参考文献
Wischang, Diana; Hartung, Jens
Tetrahedron, 2012 , vol. 68, # 46 p. 9456 - 9463
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