1-氨基-3,5-二甲苯合成路线 (共 187 条)
参考文献
Buu-Hoi; Royer
Journal of the Chemical Society, 1951 , p. 795,797
反应条件
1-methyl-pyrrolidin-2-one; sodium carbonate
24 h; Heating;
参考文献
Kubo, Yuji; Yoshida, Katsuhira; Adachi, Masafumi; Nakamura, Shinichiro; Maeda, Shuichi
Journal of the American Chemical Society, 1991 , vol. 113, # 8 p. 2868 - 2873
反应条件
potassium hydroxide in dimethyl sulfoxide
T=20 - 50°C;
参考文献
Zhang, Lei; Peng, Chen; Zhao, Dan; Wang, Yue; Fu, Hai-Jian; Shen, Qi; Li, Jian-Xin
Chemical Communications, 2012 , vol. 48, # 47 p. 5928 - 5930
反应条件
1: BF3 / Heating
2: 4.9 percent / cyclohexane / 15.5 h / Irradiation
View Scheme
参考文献
Bunce, Nigel J.; Cater, Stephen R.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 169 - 174
反应条件
1: With hydrogenchloride; sodium nitrite
T=-10°C; 0.5 h;
2: With hydrogenchloride; tin(ll) chloride
T=4°C;
参考文献
Nagarajan, K.; Talwalker, P.K.; Kulkarni, C.L.; Venkateswarlu, A.; Prabhu, S.S.; Nayak, G.V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 12 p. 1243 - 1257
反应条件
1: 1.) diazotation
2: 22 percent / N-bromosuccinimide, bezoyl peroxide / CCl4 / Heating
View Scheme
参考文献
Hoegberg, Hans-Erik; Wennerstroem, Olof
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 10 p. 661 - 668
反应条件
sodium carbonate in toluene
T=20°C; 1.5 h;
参考文献
Costa, Jorge C.S.; Neves, Josiane S.; de Souza, Marcus V.N.; Siqueira, Rodrigo A.; Romeiro, Nelilma C.; Boechat, Nubia; Silva, Patricia M.R.e; Martins, Marco A.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 3 p. 1162 - 1166