反应条件
aluminium trichloride; aluminium in 1,2,5-trimethyl-benzene
2 equiv. AlCl3, heated to 100°C, stirred under N2 for 5 h; cooled, added with stirring to ice-cold H2O, layers septd., aq. layer washed with ether and organic layer with H2O, dried (MgSO4), evapd., chromy. on alumina with light petroleum/CH2Cl2, rechromy. on silica, crystd.(MeOH or l. petroleum), elem. anal.;
参考文献
Pauson, Peter L.; Sraga, Jan; Toma, Stefan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1233 - 1236
