N-乙酰基-1,6-二氨基吡啶合成路线 （共 18 条）
反应条件
in tetrahydrofuran T=0 - 20°C; Inert atmosphereCooling with ice;
参考文献
McGrath, Jacqueline M.; Pluth, Michael D.
Journal of Organic Chemistry, 2014 , vol. 79, # 2 p. 711 - 719
反应条件
triethylamine in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
Wang, Jui-Hsu; Altukhov, Oleksii; Cheng, Chih-Chia; Chang, Feng-Chih; Kuo, Shiao-Wei
Soft Matter, 2013 , vol. 9, # 21 p. 5196 - 5206
反应条件
1: 59.4 percent / 36percent hydrochloric acid, 40percent sodium nitrite / H2O / 0.5 h 2: 69.4 percent / 10percent sulfuric acid / H2O / 0.5 h / 100 °C View Scheme
参考文献
Ferrarini; Biagi; Livi; et al.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, # 5 p. 1007 - 1010
反应条件
tetrafluoroboric acid; sodium nitrite T=-5°C; Fluorination; 1 h;
参考文献
Ferrarini, Pier Luigi; Mori, Claudio; Manera, Clementina; Mori, Filippo; Calderone, Vincenzo; Martinotti, Enrica
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 5 p. 1123 - 1127
反应条件
hydrogen bromide; sodium nitrite in water 1 h;
参考文献
Ferrarini; Biagi; Livi; et al.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, # 5 p. 1007 - 1010
反应条件
1: 61 percent / 50 percent aq. HBF4; NaNO2 / 1 h / -5 °C 2: 70 percent / 20 percent aq. H2SO4 / 4 h / 100 °C View Scheme
参考文献
Ferrarini, Pier Luigi; Mori, Claudio; Manera, Clementina; Mori, Filippo; Calderone, Vincenzo; Martinotti, Enrica
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 5 p. 1123 - 1127
反应条件
1: 13.2 percent / 36percent hydrobromic acid, 40percent sodium nitrite / H2O / 1 h 2: 80 percent / sulfuric acid / H2O View Scheme
参考文献
Ferrarini; Biagi; Livi; et al.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, # 5 p. 1007 - 1010
反应条件
hydrogenchloride; sodium nitrite in water
0.5 h;
参考文献
Ferrarini; Biagi; Livi; et al.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, # 5 p. 1007 - 1010
反应条件
triethylamine in dichloromethane
cooling;
参考文献
Nakade, Hiroshi; Ilker, M. Firat; Jordan, Brian J.; Uzun, Oktay; LaPointe, Nicholas L.; Coughlin, E. Bryan; Rotello, Vincent M.
Chemical Communications, 2005 , # 26 p. 3271 - 3273
参考文献
Ferrarini, Pier Luigi; Mori, Claudio; Primofiore, Giampaolo; Calzolari, Lorella
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 4 p. 881 - 886
