1.1: triethylamine / dichloromethane / 20 h / 20 °C 2.1: diborane / tetrahydrofuran / 2 h / 0 - 20 °C 2.2: 1 h / 0 - 20 °C 3.1: sodium hydroxide / methanol; water / 48 h / 20 °C View Scheme
参考文献
Li, Aixiao; Mishra, Yogesh; Malik, Maninder; Wang, Qi; Li, Shihong; Taylor, Michelle; Reichert, David E.; Luedtke, Robert R.; MacH, Robert H.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 11 p. 2988 - 2998
iodosylbenzene; C32H12BF24(1-)*C36H54MnN2O2(1+) in dichloromethane T=0°C; 2 h; Inert atmosphere;
参考文献
Ulmann, Pirmin A.; Braunschweig, Adam B.; Lee, One-Sun; Wiester, Michael J.; Schatz, George C.; Mirkin, Chad A.
Chemical Communications, 2009 , # 34 p. 5121 - 5123
iodosylbenzene; C32H12BF24(1-)*C36H54MnN2O2(1+) in dichloromethane T=0°C; 2 h; Inert atmosphere;
参考文献
Ulmann, Pirmin A.; Braunschweig, Adam B.; Lee, One-Sun; Wiester, Michael J.; Schatz, George C.; Mirkin, Chad A.
Chemical Communications, 2009 , # 34 p. 5121 - 5123