(1R,2R)-反-1,2-环己二醇合成路线 (共 93 条)
反应条件
cyclic dioldehydrogenase from Rhodococcus sp. Moj-3449 in aq. buffer T=30°C; pH=8; 12 h; Enzymatic reaction; enantioselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 16 p. 3147 - 3153
反应条件
sulfuric acid in ethanol 3 h; Heating;
参考文献
Itano, Kayoko; Yamasaki, Kazuo; Kihara, Chikako; Tanaka, Osamu
Carbohydrate Research, 1980 , vol. 87, p. 27 - 34
反应条件
lithium aluminium tetrahydride in diethyl ether 6 h; Heating;
参考文献
Tetrahedron Asymmetry, , vol. 7, # 11 p. 3285 - 3294
反应条件
1: 42 percent / phosphate buffer (pH 7.0) / H2O / 8 h / 30 °C / Pseudomonas fluorescens lipase (Amano P) 2: 100 percent / K2CO3 / methanol View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 2, # 5 p. 389 - 398
反应条件
C42H60N6O7; benzyl alcohol; cyclohexanol; butan-1-ol in toluene T=0°C; 1 h;
参考文献
Mueller, Christian E.; Zell, Daniela; Hrdina, Radim; Wende, Raffael C.; Wanka, Lukas; Schuler, Soeren M. M.; Schreiner, Peter R.
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8465 - 8484
反应条件
C43H60N6O8; N-ethyl-N,N-diisopropylamine in toluene T=0°C; 24 h; Inert atmosphere; enantioselective reaction;
参考文献
Chemical Communications, , vol. 50, # 10 p. 1221 - 1223
反应条件
C43H60N6O8; N-ethyl-N,N-diisopropylamine in toluene T=0°C; 24 h; Inert atmosphere; enantioselective reaction;
参考文献
Chemical Communications, , vol. 50, # 10 p. 1221 - 1223
反应条件
C43H60N6O8; N-ethyl-N,N-diisopropylamine in toluene T=0°C; 48 h; Inert atmosphere; enantioselective reaction;
参考文献
Chemical Communications, , vol. 50, # 10 p. 1221 - 1223
反应条件
C43H60N6O8; N-ethyl-N,N-diisopropylamine in toluene T=0°C; 6 h; Inert atmosphere; enantioselective reaction;
参考文献
Chemical Communications, , vol. 50, # 10 p. 1221 - 1223
反应条件
1: trans-1,2-cyclohexanediol With potassium phosphate; (S)-2-methoxy-2-phenylacetic acid; C18H16N3O(1+)*(x)BF4 in chloroform T=20°C; 0.166667 h; 2: 2-bromo-3-phenylpropanal in chloroform T=20°C; 12 h; Reagent/catalyst;
参考文献
Journal of the American Chemical Society, , vol. 135, # 31 p. 11485 - 11488