1: 4-Methylpyridine With n-butyllithium in tetrahydrofuran T=-78 - 45°C; 2 h; 2: 1-bromo-3-methyl-butane in tetrahydrofuran T=-78 - 20°C; 3: With water in tetrahydrofuran
参考文献
THE UNIVERSITY OF SYDNEY
Patent: WO2007/128059 A1, 2007 ;
Location in patent: Page/Page column 24 ;
WO 2007/128059 A1
1: 1-bromo-3-methyl-butane With magnesium in tetrahydrofuran Heating; 2: 1-Bromo-11-hydroxyundecane With lithium chloride; copper dichloride in tetrahydrofuran T=-78 - 20°C; Further stages.;
参考文献
Mun, JiYoung; Onorato, Amber; Nichols, Frank C.; Morton, Martha D.; Saleh, Abdullah I.; Welzel, Morgan; Smith, Michael B.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 23 p. 3826 - 3833
