4-甲氧基-4-甲基-2-戊酮合成路线 (共 18 条)
反应条件
N,N',N''-tris(p-tolyl)azacalix[3](2,6)(4-pyrrolidinopyridine) in neat liquid T=50°C; 12 h; Inert atmosphere;
参考文献
Uchida, Natsuko; Kuwabara, Junpei; Taketoshi, Ayako; Kanbara, Takaki
Journal of Organic Chemistry, 2012 , vol. 77, # 23 p. 10631 - 10637
反应条件
dodecacarbonyltetrarhodium(0) in benzene T=100°C; 17 h;
参考文献
Sato, Susumu; Matsuda, Isamu; Izum, Yusuke
Tetrahedron Letters, 1987 , vol. 28, # 52 p. 6657 - 6660
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Sato, Susumu; Matsuda, Isamu; Izumi, Yusuke
Journal of Organometallic Chemistry, 1988 , vol. 352, p. 223 - 238
反应条件
toluene-4-sulfonic acid in methanol T=0°C; 5 h;
参考文献
Chemistry Letters, , vol. 38, # 1 p. 96 - 97
反应条件
Tl(NO3)3*3H2O in methanol; dichloromethane 1 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 997 - 1000
反应条件
Tl(NO3)3*3H2O in methanol; dichloromethane 1 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 997 - 1000
反应条件
silver perchlorate 0.25 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 40, # 2 p. 315 - 326
反应条件
C41H58ClN4Ru(1+)*Cl(1-); isopropyl alcohol; potassium hydroxide T=82°C; 0.5 h;
参考文献
Goek, Luetfiye; Tuerkmen, Hayati
Tetrahedron, 2013 , vol. 69, # 49 p. 10669 - 10674
反应条件
ammonium chloride 1) THF, -78 deg C to 20 deg C, 18 h; Yield given. Multistep reaction;
参考文献
Kauffmann, Thomas; Neiteler, Christel; Robbe, Sonja
Chemische Berichte, 1992 , vol. 125, # 11 p. 2409 - 2418
反应条件
hydrazine hydrate Behandeln des Reaktionsprodukts mit HCN und anschliessend mit wss.-aethanol.HCl und Chlor; optically inactive stereoisomer(ic) of mp: 58 degree;
参考文献
Du Pont de Nemours and Co.
Patent: US2586995 , 1948 ;
反应条件
aluminium trichloride; ammonia
1.) 35 deg C, 1 h; Yield given. Multistep reaction. Further byproducts given;
参考文献
Erre, Claude H.; Roussel, Christian
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 11-12 p. 454 - 457