in 1,4-dioxane
byproducts: Me3SiCl, Me3SiOSiMe2OSiMe3, Me3SiOSiMe2Cl; mixt. of dichlorogermylene and siloxane in dioxane stirred for 29 h at 85-95°C with barbotage of air, further products; liq. phase distilled at atm. pressure and in vaq.;
参考文献
Shcherbinin; Pushkina; Krivolapova; Bykovchenko; Khromykh; Komalenkova; Chernyshev
Russian Journal of General Chemistry, 2002 , vol. 72, # 12 p. 1907 - 1910
in 1,4-dioxane
byproducts: Me3SiCl, Me3SiOSiMe2OSiMe3, Me3SiOSiMe2Cl; mixt. of dichlorogermylene and siloxane in dioxane stirred for 80-90 h at 85-95°C; liq. phase distilled at atm. pressure and in vaq.;
参考文献
Shcherbinin; Pushkina; Krivolapova; Bykovchenko; Khromykh; Komalenkova; Chernyshev
Russian Journal of General Chemistry, 2002 , vol. 72, # 12 p. 1907 - 1910
in 1,4-dioxane
byproducts: Me3SiCl, Me3SiOSiMe2OSiMe3, Me3SiOSiMe2Cl; mixt. of dichlorogermylene and siloxane in dioxane stirred for 29 h at 85-95°C with barbotage of air; liq. phase distilled at atm. pressure and in vaq.;
参考文献
Shcherbinin; Pushkina; Krivolapova; Bykovchenko; Khromykh; Komalenkova; Chernyshev
Russian Journal of General Chemistry, 2002 , vol. 72, # 12 p. 1907 - 1910
Lohmeijer, Bas G. G.; Dubois, Geraud; Leibfart, Frank; Pratt, Russell C.; Nederberg, Fredrik; Nelson, Alshakim; Waymouth, Robert M.; Wade, Charles; Hedrick, James L.
Organic Letters, 2006 , vol. 8, # 21 p. 4683 - 4686
