反应条件
in neat (no solvent) byproducts: CH3OSi(CH3)3; MeO(Me)BC(SiMe3) was sublimed into a tube heated at 560°C within 2 h, products of thermolysis were condensed at -198°C in pentane; volatiles were removed in vac. at -40°C, mixt. was recondensed at 25°C and 0,001 Torr, but not sepd.; identified by NMR;
参考文献
Chemische Berichte, , vol. 122, p. 1057 - 1060