反应条件
in neat (no solvent) byproducts: (C2H5)2PbCl2, (C2H5)4Pb; mixt. heated at 150°C for 15 h in a sealed evacuated ampoule; volatiles removed (vac., 100°C) and collected in a trap, residue treated with heptane, cooled to -5°C (crystn.);
参考文献
Shcherbakov, V. I.; Stolyarova, N. E.; Konkina, T. N.
Journal of General Chemistry USSR (English Translation), 1987 , vol. 57, p. 1466 - 1469
Zhurnal Obshchei Khimii, 1987 , vol. 57, p. 1643 - 1647