反应条件
in dichloromethane N2 atmosphere, addn. of soln. of stannyl compound to soln. of borane at -78°C (3 h) with stirring, slow warming to room temp., stirring (room temp., 17 h); removement of solvent (25°C, 13 Torr) and Me3SnBr (30°C, 1E-2 Torr or 53-55°C, 12 Torr), distillation (63-66°C, 1E-5Torr), cryst.; elem. anal.;
参考文献
Diemer, Stefan; Noeth, Heinrich; Storch, Wolfgang
European Journal of Inorganic Chemistry, 1999 , # 9 p. 1765 - 1780
