potassium hydroxide; sodium dithionite
unter Stickstoff; Erwaermen des Reaktionsprodukts in 2,4-Dimethyl-pentan-3-on mit wss. Natronlauge und wenig Natriumdithionit.;
Manoharan, T. S.; Madyastha, K.M.; Singh, B. B.; Bhatnagar, S. P.; Weiss, U.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 6 p. 558 - 559
n-butyllithium
1) in hexane, tetrahydrofuran, -78 deg C, 5 min 2) 0.5 h, -78 deg C, then -10 deg C; Yield given. Multistep reaction. Further byproducts given. Title compound not separated from byproducts;
参考文献
Sanghvi, Y. S.; Dabral, V.; Bhat, K. S.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 1 p. 12 - 14
n-butyllithium
1) in hexane, tetrahydrofuran, -78 deg C, 5 min 2) 0.5 h, -78 deg C, then -10 deg C; Multistep reaction. Further byproducts given. Title compound not separated from byproducts;
参考文献
Sanghvi, Y. S.; Dabral, V.; Bhat, K. S.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 1 p. 12 - 14
