2,6-二甲基-5-庚烯醛合成路线 （共 18 条）
反应条件
dihydrogen peroxide in water; 1,2-dichloro-ethane Baeyer-Villiger Ketone Oxidation; 4 h; Reflux;
参考文献
US2014/128622 A1, ;
Paragraph 0214-0215 ;
反应条件
potassium hydride in tetrahydrofuran 1 h; Heating;
参考文献
Takano, Seiichi; Satoh, Shigeki; Ogasawara, Kunio
Heterocycles, 1985 , vol. 23, # 1 p. 41 - 44
反应条件
in benzene T=0°C; Elimination; 0.5 h; Photolysis;
参考文献
Journal of Organic Chemistry, , vol. 65, # 8 p. 2292 - 2304
反应条件
bromine 2.) THF, 2.) 25 deg C, 30 min;
参考文献
Lozanova, A. V.; Gul'tyai, V. P.; Karaseva, A. N.; Moiseenkov, A. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, p. 1241 - 1245
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 6 p. 1370 - 1373
反应条件
oxalyl dichloride; dimethyl sulfoxide; triethylamine Yield given. Multistep reaction;
参考文献
Chemical Communications, , # 15 p. 1531 - 1532
反应条件
1: 1.) OsO4, NMO, H2O, 2.) NaIO4, H2O / 1.) acetone, 2.) THF 3: Na, liq. NH3 4: 1.) (COCl)2, DMSO, 2.) Et3N View Scheme
参考文献
Chemical Communications, , # 15 p. 1531 - 1532
反应条件
2: Na, liq. NH3 3: 1.) (COCl)2, DMSO, 2.) Et3N View Scheme
参考文献
Chemical Communications, , # 15 p. 1531 - 1532
反应条件
tin; dihydrogen peroxide in various solvent(s) T=100°C; Baeyer-Villiger oxidation; 1 h; Product distribution; Further Variations:SolventsTemperaturesReagents;
参考文献
Journal of Catalysis, , vol. 234, # 1 p. 96 - 100
参考文献
Bulletin de la Societe Chimique de France, , vol. <4>45, p. 712
参考文献
Bulletin de la Societe Chimique de France, , vol. <4>45, p. 712
