1: carbon disulfide; isopropylamine With sodium hydroxide in water T=100°C; Microwave irradiation; 2: chloroacetic acid in water T=100°C; 0.0833333 h; Microwave irradiation; 3: With hydrogenchloride in water T=120°C; 0.5 h; Microwave irradiation;
参考文献
Nitsche, Christoph; Schreier, Verena N.; Behnam, Mira A. M.; Kumar, Anil; Bartenschlager, Ralf; Klein, Christian D.
Journal of Medicinal Chemistry, 2013 , vol. 56, # 21 p. 8389 - 8403
1: carbon disulfide; isopropylamine in neat (no solvent) T=20°C; 0.0333333 h; Green chemistry; 2: chloroacetyl chloride in neat (no solvent) 0.0833333 h; Green chemistry;
参考文献
Nasiri, Farough; Zolali, Amin; Azimian, Zeinab
Journal of Sulfur Chemistry, 2014 , vol. 35, # 1 p. 62 - 66