5-乙酰氧基甲基-2-呋喃醛合成路线 （共 47 条）
反应条件
pyridine in acetonitrile T=20°C; 3 h; Inert atmosphere;
参考文献
The Board of Trustees of the University of Illinois
Patent: US2011/263880 A1, 2011 ;
Location in patent: Page/Page column 13 ;
反应条件
potassium carbonate in acetonitrile T=20°C; 5 h;
参考文献
Kim, Jung-Keun; Kim, Se-Won; Oh, Kwi-Ok; Ko, Seon Yle; Kim, Jong Yeo; Lee, Byung-Eui; Kim, Bum Tae; Lee, Yeon Soo; Min, Yong Ki; Park, No Kyun
Patent: US2008/221205 A1, 2008 ;
Location in patent: Page/Page column 5-6 ;
反应条件
zirconium tetraacetate; acetaldehyde; sodium bromide; Co(II)-Mn(II) acetate T=75°C; 5.16667 h; KineticsProduct distribution; Further Variations:CatalystsTemperaturesPressuresratio;
参考文献
Partenheimer, Walt; Grushin, Vladimir V.
Advanced Synthesis and Catalysis, 2001 , vol. 343, # 1 p. 102 - 111
反应条件
chromium dichloride in 1-ethyl-3-methyl-1H-imidazolium chloride T=100°C; P=9375.94 Torr; 3 h; Product distribution / selectivity;
参考文献
WO2009/30512 A2, ;
Page/Page column 7 ;
反应条件
1: fructose powder With acetic acid; magnesium chloride in water T=75 - 95°C; 4.5 h; 2: acetic anhydride With 4-(N,N-dimethlyamino)pyridine in acetic acid T=20 - 80°C; Product distribution / selectivity;
参考文献
EVONIK DEGUSSA GmbH
Patent: US2008/200698 A1, 2008 ;
Location in patent: Page/Page column 6 ;
反应条件
chromium dichloride in H-3-methylimidazolium bis(trifluoromethanesulfonyl)imide; 1-ethyl-3-methyl-1H-imidazolium chloride T=100°C; P=9375.94 Torr; 3 h; Product distribution / selectivity;
参考文献
WO2009/30512 A2, ;
Page/Page column 7 ;
反应条件
pyridine in dichloromethane
反应条件
trichlorophosphate in 1,2-dichloro-ethane T=20°C; Vilsmeier-Haack reaction; 24 h;
参考文献
Mehner, Alexander; Montero, Ana L.; Martinez, Ricardo; Spange, Stefan
Molecules, 2007 , vol. 12, # 3 p. 634 - 640
反应条件
Amberlyst 35 in water T=80°C; Product distribution / selectivity;
参考文献
SANBORN, Alexandra J.; Howard, Stephen J.
Patent: US2009/156841 A1, 2009 ;
Location in patent: Page/Page column 6-9 ;
反应条件
Amberlyst 15 T=110 - 125°C; 2 - 3 h; Product distribution / selectivity;
参考文献
US2009/156841 A1, ;
Page/Page column 9 ;
