[二(苯基)磷酰-苯基磷酰]苯合成路线 (共 17 条)
反应条件
in dimethyl sulfoxide 0.5 h; Irradiation;
参考文献
Russell, Glen A.; Khanna, Rajive K.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 29, p. 271 - 274
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; Inert atmosphere; 2: With 2-methyl-5,8-dioxo-5,8-dihydroquinoline-7-amine in tetrahydrofuran; hexane T=20°C; 3 h; Inert atmosphere;
参考文献
Nycz, Jacek E.; Malecki, Grzegorz; Chikkali, Samir; Hajdok, Imre; Singh, Priti
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 5 p. 564 - 572
反应条件
oxygen in benzene T=0°C;
参考文献
Lindner, Ekkehard; Kern, Herbert
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1983 , vol. 38, # 6 p. 790 - 792
反应条件
samarium diiodide in tetrahydrofuran 0.583333 h; Ambient temperature;
参考文献
Sasaki, Mitsuru; Collin, Jacqueline; Kagan, Henri B.
Tetrahedron Letters, 1991 , vol. 32, # 22 p. 2493 - 2496
反应条件
lithium amalgam in tetrahydrofuran 1.) r.t., 2.) reflux, 15 min;
参考文献
Horner, Leopold; Dickerhof, Karlheinz
Chemische Berichte, 1983 , vol. 116, # 4 p. 1603 - 1614
反应条件
18-crown-6 ether in dimethyl sulfoxide 0.5 h; Irradiation;
参考文献
Russell, Glen A.; Khanna, Rajive K.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 29, p. 271 - 274
反应条件
1: potassium naphthalenide / tetrahydrofuran / -78 °C 2: 1.408 g / tetrahydrofuran / 16 h / -78 °C View Scheme
参考文献
Nycz, Jacek E.; Musiol, Robert
Heteroatom Chemistry, 2006 , vol. 17, # 4 p. 310 - 316
反应条件
1: 47 percent / 18-crown-6 / hexamethylphosphoric acid triamide / 0.5 h / Irradiation 2: 72 percent / dimethylsulfoxide / 0.5 h / Irradiation View Scheme
参考文献
Russell, Glen A.; Khanna, Rajive K.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 29, p. 271 - 274
反应条件
in tetrahydrofuran T=-78°C; 16 h;
参考文献
Nycz, Jacek E.; Musiol, Robert
Heteroatom Chemistry, 2006 , vol. 17, # 4 p. 310 - 316
反应条件
oxygen in diethyl ether T=0°C; reactions in other solvents to the same or other products; MechanismProduct distribution;
参考文献
Lindner, Ekkehard; Kern, Herbert
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1983 , vol. 38, # 6 p. 790 - 792