(Z)-3,7-二甲基-2,6-亚辛基-1-醇丙酸酯合成路线 （共 8 条）
反应条件
propionic acid sodium salt in chlorobenzene P=760.051 Torr; 17 h; Heating / reflux;
参考文献
LOYOLA UNIVERSITY OF CHICAGO
Patent: WO2005/44774 A1, 2005 ;
Location in patent: Page/Page column 15-16 ;
反应条件
triethylamine in diethyl ether T=0°C; 1 h;
参考文献
Novak, Lajos; Poppe, Laszlo; Kis-Tamas, Attila; Szantay, Csaba
Acta Chimica Hungarica, 1985 , vol. 118, # 1 p. 17 - 24
反应条件
Candida antarctica lipase B T=50°C; 4 h; Molecular sieveIonic liquidGreen chemistryEnzymatic reaction;
参考文献
Lozano, Pedro; Bernal, Juana M.; Navarro, Alicia
Green Chemistry, 2012 , vol. 14, # 11 p. 3026 - 3033
反应条件
methanesulfonyl chloride; triethylamine in dichloromethane T=-5°C; 0.666667 h; Yield given. Yields of byproduct given;
参考文献
Novak, Lajos; Poppe, Laszlo; Kis-Tamas, Attila; Szantay, Csaba
Acta Chimica Hungarica, 1985 , vol. 118, # 1 p. 17 - 24
反应条件
1: 52 percent / Et3N / diethyl ether / 0.33 h / 0 °C 2: Et3N, MsCl / CH2Cl2 / 0.67 h / -5 °C View Scheme
参考文献
Novak, Lajos; Poppe, Laszlo; Kis-Tamas, Attila; Szantay, Csaba
Acta Chimica Hungarica, 1985 , vol. 118, # 1 p. 17 - 24
反应条件
1: 90 percent / LiAlH4 / diethyl ether / 0.5 h / Heating 2: 52 percent / Et3N / diethyl ether / 0.33 h / 0 °C 3: Et3N, MsCl / CH2Cl2 / 0.67 h / -5 °C View Scheme
参考文献
Novak, Lajos; Poppe, Laszlo; Kis-Tamas, Attila; Szantay, Csaba
Acta Chimica Hungarica, 1985 , vol. 118, # 1 p. 17 - 24
反应条件
potassium carbonate; 3-chloro-benzenecarboperoxoic acid in dichloromethane
参考文献
Novak, Lajos; Poppe, Laszlo; Kis-Tamas, Attila; Szantay, Csaba
Acta Chimica Hungarica, 1985 , vol. 118, # 1 p. 17 - 24
反应条件
1: 85 percent / K2CO3, MCPBA / CH2Cl2
2: 90 percent / LiAlH4 / diethyl ether / 0.5 h / Heating
View Scheme
参考文献
Novak, Lajos; Poppe, Laszlo; Kis-Tamas, Attila; Szantay, Csaba
Acta Chimica Hungarica, 1985 , vol. 118, # 1 p. 17 - 24
