styryltriphenylphosphonium chloride in 1,2-dichloro-ethane byproducts: 1-propenyltriphenylphosphonium chloride, 1-choro-1-propene; evacuated and N2 added two times; dichloroethane addn.; evacuated until boiled at room temp., and N2 added rapidly; cycle repeated; cooled to -78°C, tube sealed; reflux 1 h; decane added; distd. volatiles; from residue recrystd. at -10°C;;
参考文献
Kampmeier, J. A.; Harris, S. H.; Rodehorst, R. M.
Journal of the American Chemical Society, 1981 , vol. 103, # 6 p. 1478 - 1485
Young; Eisner
Journal of the American Chemical Society, 1941 , vol. 63, p. 2114
Full Text Show Details
Young; Winstein; Prater
Journal of the American Chemical Society, 1936 , vol. 58, p. 290