1,1'-联(环己烷)-1'-烯-2-胺合成路线 （共 35 条）
反应条件
ytterbium(III) triflate; bis(η5-cyclopentadienyl)MoH2 in methanol T=50°C; 24 h;
参考文献
Journal of Organometallic Chemistry, , vol. 569, # 1-2 p. 139 - 145
反应条件
sodium tetrahydroborate; nickel boride in methanol Yield given;
参考文献
Tetrahedron Letters, , vol. 26, # 52 p. 6413 - 6416
反应条件
potassium; carbon in tetrahydrofuran
参考文献
Savoia,D. et al.
Journal of Organic Chemistry, 1978 , vol. 43, p. 2907 - 2910
反应条件
(i) EtMgBr, THF, (ii) /BRN= 1420755/, (iii) aq. HCl; Multistep reaction;
参考文献
Cuvigny,T.; Normant,H.
Organometallics in Chemical Synthesis, 1971 , vol. 1, p. 237 - 247
反应条件
(i) EtMgBr, THF, (ii) /BRN= 507487/, (iii) aq. HCl; Multistep reaction;
参考文献
Destabel, Christine; Kilburn, Jeremy D.; Knight, John
Tetrahedron, 1994 , vol. 50, # 38 p. 11267 - 11288
反应条件
1: (i) Li, Et2NH, HMPT, (ii) /BRN= 906754/, (iii) aq. HCl
2: H2SO4
View Scheme
参考文献
Larcheveque,M. et al.
Synthesis, 1977 , p. 424 - 427
反应条件
1: (i) LDA, THF, (ii) /BRN= 1698609/, HMPT, (iii) tartaric acid, H2O
2: AcOH / H2O / 2 h / Ambient temperature
View Scheme
参考文献
Larcheveque,M. et al.
Tetrahedron, 1979 , vol. 35, p. 1745 - 1749
反应条件
2: via 2,6-dibromo derivative
3: 81 percent / O2 / CuCl2
View Scheme
参考文献
Utaka, Masanori; Watabu, Hisashi; Takeda, Akira
Chemistry Letters, 1985 , p. 1475 - 1476
反应条件
lithium diisopropyl amide in tetrahydrofuran
T=0°C; 0.75 h;
参考文献
Fleming, Ian; Goldhill, Jon; Perry, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 7 p. 1563 - 1570
反应条件
sodium hydrogen sulphate in water
1 h;
参考文献
Troyanskii, E. A.; Ioffe, V. A.; Mizintsev, V. V.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1661 - 1667
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 8 p. 1814 - 1822
