1-甲基吡咯烷-2-硫酮合成路线 （共 20 条）
反应条件
1: 90 percent / CH2Cl2 / 0.5 h / Ambient temperature 2: 87 percent / KF / Triethylbenzylammonium chloride / CH2Cl2 / 6 h / Ambient temperature View Scheme
参考文献
Singh, Harjit; Batra, M. S.; Singh, Paramjit
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 12 p. 1176 - 1180
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=0°C; 2 h;
参考文献
Kochhar, Kanwarpal S.; Cottrell, David A.; Pinnick, Harold W.
Tetrahedron Letters, 1983 , vol. 24, # 13 p. 1323 - 1326
反应条件
tert-butylhypochlorite in tetrachloromethane T=25°C; 0.5 h;
参考文献
Tetrahedron, , vol. 39, # 10 p. 1729 - 1734
反应条件
sodium monomethylcarbonate; silver carbonate in tetrahydrofuran 2 h;
参考文献
Brillon, Denis; Sauve, Gilles
Journal of Organic Chemistry, 1990 , vol. 55, # 7 p. 2246 - 2249
反应条件
Lawesson's reagent in dichloromethane
T=20°C; 2 h;
参考文献
Koduri, Naga Durgarao; Scott, Halee; Hileman, Bethany; Cox, Justin D.; Coffin, Michael; Glicksberg, Lindsay; Hussaini, Syed R.
Organic Letters, 2012 , vol. 14, # 2 p. 440 - 443
反应条件
MCM-41 mesoporous silica in ethanol; water
T=80 - 90°C; 8 h; Green chemistry;
参考文献
Ray, Suman; Bhaumik, Asim; Dutta, Arghya; Butcher, Ray J.; Mukhopadhyay, Chhanda
Tetrahedron Letters, 2013 , vol. 54, # 17 p. 2164 - 2170
反应条件
sodium hydrogensulfide in acetone
T=0°C;
参考文献
Kaloustian, Moses K.; Nader, Randa B.
Journal of Organic Chemistry, 1981 , vol. 46, # 24 p. 5050 - 5052
反应条件
sodium hydrogensulfide in acetone
T=0°C;
参考文献
Bodine, John J.; Kaloustian, Moses K.
Synthetic Communications, 1982 , vol. 12, # 10 p. 787 - 794
反应条件
bis(trimethylsilyl)-sulfide in dichloromethane
4 h; Ambient temperature; Yield given;
参考文献
Smith, D. C.; Lee, S. W.; Fuchs, P. L.
Journal of Organic Chemistry, 1994 , vol. 59, # 2 p. 348 - 354
反应条件
sodium hydrogensulfide in chloroform
Heating; Yield given. Yields of byproduct given;
参考文献
Kaloustian, Moses K.; Nader, Randa B.
Journal of Organic Chemistry, 1981 , vol. 46, # 24 p. 5050 - 5052
