1: KH / tetrahydrofuran 2: n-BuLi / tetrahydrofuran; hexane / 0.33 h / 0 - 5 °C 3: tetrahydrofuran / 4 h / Ambient temperature; var. alkyl halides, C-1/C-3 ratio of alkylated products View Scheme
参考文献
Trimitsis, G. B.; Hinkley, J. M.; TenBrink, R.; Faburada, A. L.; Anderson, R.; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 18 p. 2957 - 2962
methanesulfonic acid; (R,R)-dihydroborate in hexane T=-20°C; 48 h; Title compound not separated from byproducts;
参考文献
Imai, Toshiro; Tamura, Tadashi; Yamamuro, Akira; Sato, Tsuneo; Wollmann, Theodor A.; et al.
Journal of the American Chemical Society, 1986 , vol. 108, # 23 p. 7402 - 7404