反式-1,2-二苯乙烯合成路线 (共 348 条)
反应条件
sulfur T=425°C; P=760 Torr; var. time; Product distribution;
参考文献
Stenberg, Virgil I.; Hei, Robert D.
Journal of Organic Chemistry, 1985 , vol. 50, # 11 p. 1810 - 1815
反应条件
in tetrahydrofuran 3 h; Ambient temperatureIrradiation; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 55, # 15 p. 4537 - 4544
反应条件
Oxonereg;; (ethylenedinitrilo)tetraacetic acid disodium salt; sodium hydrogencarbonate in water; acetonitrile Ambient temperature;
参考文献
Yang, Dan; Yip, Yiu-Chung; Jiao, Guan-Sheng; Wong, Man-Kin
Journal of Organic Chemistry, 1998 , vol. 63, # 24 p. 8952 - 8956
反应条件
oxygen T=100°C; P=760.051 Torr; 24 h;
参考文献
Chemical Communications, , vol. 46, # 45 p. 8591 - 8593
反应条件
1: Fe(II), H2O2 / acetonitrile 2: Fe(II), H2O2 / acetonitrile; H2O / pH 4 View Scheme
参考文献
Sugimoto, Hiroshi; Sawyer, Donald T.
Journal of the American Chemical Society, 1984 , vol. 106, # 15 p. 4283 - 4285
反应条件
TPPP; (+)-N-{(4S,5S)-2,2-dimethyl-4-[4-(methylsulfonyl)phenyl]-1,3-dioxan-5-yl}-3,4-dihydroisoquinolinium tetraphenylborate in acetonitrile T=-40°C; 24 h; Product distribution / selectivity;
参考文献
AVECIA PHARMACEUTICALS LIMITED
Patent: WO2005/56543 A2, 2005 ;
Location in patent: Page/Page column 29-30 ;
反应条件
di-tert-butyl peroxide 24 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 49, # 23 p. 4482 - 4486
反应条件
N-methyl-2-indolinone; fluorous OsO4 in water; acetone; tert-butyl alcohol T=20°C; 36 h;
参考文献
Huang, Yangen; Meng, Wei-Dong; Qing, Feng-Ling
Tetrahedron Letters, 2004 , vol. 45, # 9 p. 1965 - 1968
反应条件
in water; acetone; acetonitrile
参考文献
Council of Scientific and Industrial Research
Patent: US6552234 B1, 2003 ;
反应条件
tert.-butylhydroperoxide; osmium(VIII) oxide in water; toluene; acetonitrile T=0°C;
参考文献
Journal of Organic Chemistry, , vol. 59, # 6 p. 1375 - 1380