2-(乙基硫代)-1-苯基乙酮合成路线 (共 20 条)
反应条件
potassium carbonate; Aliquatreg; 336 in toluene T=20°C; 4 h;
参考文献
Lissel, Manfred
Journal of Chemical Research, Miniprint, 1982 , # 10 p. 2946 - 2966
反应条件
1: ethanethiol With sodium methylate in methanol 0.0833333 h; Inert atmosphere; 2: α-bromoacetophenone in methanol Inert atmosphere;
参考文献
Su, Qiong; Zhao, Zi-Jian; Xu, Feng; Lou, Peng-Cai; Zhang, Kai; Xie, De-Xun; Shi, Lei; Cai, Qing-Yun; Peng, Zhi-Hong; An, De-Lie
European Journal of Organic Chemistry, 2013 , # 8 p. 1551 - 1557
反应条件
sodium hydroxide in ethanol T=20°C; 0.916667 h;
参考文献
Yu, Haifeng; Dong, Dewen; Ouyang, Yan; Wang, Yan; Liu, Qun
Synlett, 2007 , # 1 p. 151 - 155
反应条件
t-Bu-XantPhos; dichloro bis(acetonitrile) palladium(II); potassium carbonate; cesium fluoride; 4-ethynyl-1-methoxy-benzene in toluene T=100°C; 20 h; Inert atmosphere;
参考文献
Liu, Yan-Yun; Yang, Xu-Heng; Huang, Xiao-Cheng; Wei, Wen-Ting; Song, Ren-Jie; Li, Jin-Heng
Journal of Organic Chemistry, 2013 , vol. 78, # 20 p. 10421 - 10426
反应条件
1: 2-acetyl-3,3-bis-ethylsulfanyl-N-o-tolyl-acrylamide With sodium hydroxide in ethanol T=25°C; 0.833333 h; 2: α-bromoacetophenone in ethanol T=25°C;
参考文献
Yu, Haifeng
Chinese Journal of Chemistry, 2012 , vol. 30, # 2 p. 367 - 371
反应条件
1: α-bromoacetophenone With 1,4-diaza-bicyclo[2.2.2]octane in water T=20°C; 2: With potassium carbonate in water T=20°C; 3: EtSCN in water Reflux;
参考文献
Kianmehr, Ebrahim; Mirza Agha, Mansoureh; Estiri, Hamid
Monatshefte fur Chemie, 2010 , vol. 141, # 4 p. 409 - 411
反应条件
[C4mim][OH] T=20°C; 0.166667 h;
参考文献
Ranu, Brindaban C.; Mandal, Tanmay; Banerjee, Subhash; Dey, Suvendu S.
Australian Journal of Chemistry, 2007 , vol. 60, # 4 p. 278 - 283
反应条件
sodium ethanolate; ethyl mercaptan sodium salt in ethanol T=25°C; 2 h;
参考文献
Grossert, J. Stuart; Dubey, Pramod K.
Journal of the Chemical Society, Chemical Communications, 1982 , # 20 p. 1183 - 1184
反应条件
sodium ethanolate; ethyl mercaptan sodium salt in ethanol T=25°C; 2 h;
参考文献
Grossert, J. Stuart; Dubey, Pramod K.
Journal of the Chemical Society, Chemical Communications, 1982 , # 20 p. 1183 - 1184
反应条件
aluminium trichloride
参考文献
Long
Journal of the American Chemical Society, 1946 , vol. 68, p. 2159