2-(4-乙酰基苯基)乙腈合成路线 （共 14 条）
反应条件
tris(dibenzylideneacetone)dipalladium (0); ZnF2; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=90°C; 8 h;
参考文献
Wu, Lingyun; Hartwig, John F.
Journal of the American Chemical Society, 2005 , vol. 127, # 45 p. 15824 - 15832
反应条件
in 1,4-dioxane; water T=90°C; 2 h;
参考文献
Pieck, J. Carsten; Kuch, David; Grolle, Friederike; Linne, Uwe; Haas, Clemens; Carell, Thomas
Journal of the American Chemical Society, 2006 , vol. 128, # 5 p. 1404 - 1405
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; water in dimethyl sulfoxide T=130°C; Domino Suzuki coupling and fragmentation reaction; 16 h; Inert atmosphere;
参考文献
Velcicky, Juraj; Soicke, Arne; Steiner, Roland; Schmalz, Hans-Guenther
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 6948 - 6951
反应条件
1: 95 percent / NBS; AIBN / acetonitrile / 1.5 h / 90 °C 2: 67 percent / dioxane; H2O / 2 h / 90 °C View Scheme
参考文献
Xu; Wan
Chemical Communications, 2000 , # 21 p. 2147 - 2148
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; bis(η3-allyl-μ-chloropalladium(II)) in 1,3,5-trimethyl-benzene T=20 - 140°C; 5.16667 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Shang, Rui; Ji, Dong-Sheng; Chu, Ling; Fu, Yao; Liu, Lei
Angewandte Chemie - International Edition, 2011 , vol. 50, # 19 p. 4470 - 4474
反应条件
1: aqueous HCl 2: LiAlH4; diethyl ether 3: aqueous methanol.HCl 4: SOCl2; benzene 5: aqueous ethanol View Scheme
参考文献
Schmid et al.
Monatshefte fuer Chemie, 1952 , vol. 83, p. 185,187
反应条件
1: SOCl2; benzene 2: aqueous ethanol View Scheme
参考文献
Schmid et al.
Monatshefte fuer Chemie, 1952 , vol. 83, p. 185,187
反应条件
1: aqueous methanol.HCl 2: SOCl2; benzene 3: aqueous ethanol View Scheme
参考文献
Schmid et al.
Monatshefte fuer Chemie, 1952 , vol. 83, p. 185,187
反应条件
1: LiAlH4; diethyl ether 2: aqueous methanol.HCl 3: SOCl2; benzene 4: aqueous ethanol View Scheme
参考文献
Schmid et al.
Monatshefte fuer Chemie, 1952 , vol. 83, p. 185,187
参考文献
Schmid et al.
Monatshefte fuer Chemie, 1952 , vol. 83, p. 185,187
