copper(l) iodide; C14H24N2O; methyl iodide in tetrahydrofuran; hexane T=-78°C; 1.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 108, # 22 p. 7114 - 7116
1: With diphenyl-N,N-bis-((S,S)-1-naphthalen-2-yl-ethyl)phosphinamine; copper(ll) bromide in diethyl ether T=-30°C; 3 h; 2: With ammonium chloride in diethyl ether; water optical yield given as percent eeenantioselective reaction;