(2-甲基-1,2,3,4-四氢-4-喹啉)-苯胺合成路线 (共 10 条)
反应条件
1: acetaldehyde; aniline With boron trifluoride diethyl etherate in toluene T=-78°C; 0.166667 h; 2: phenylvinylamine in toluene 0.5 h;
参考文献
CARE X S.A.
Patent: WO2004/72041 A1, 2004 ;
Location in patent: Page/Page column 79-80 ;
反应条件
hydrogenchloride; titanium(III) chloride in acetic acid T=45°C; 1 h; or with the diazonium fluoroborate;
参考文献
Clerici; Porta
Tetrahedron Letters, 1990 , vol. 31, # 14 p. 2069 - 2072
反应条件
hydrogenchloride; titanium(III) chloride in acetic acid T=45°C; 1 h; or with the diazonium fluoroborate;
参考文献
Clerici; Porta
Tetrahedron Letters, 1990 , vol. 31, # 14 p. 2069 - 2072
反应条件
hydrogenchloride; titanium(III) chloride in acetic acid 1 h; Ambient temperatureor with the diazonium fluoroborate;
参考文献
Clerici; Porta
Tetrahedron Letters, 1990 , vol. 31, # 14 p. 2069 - 2072
反应条件
T=30°C; 1 h; UV-irradiationInert atmosphere;
参考文献
Selvam; Swaminathan
Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, 2013 , vol. 43, # 4 p. 500 - 508
参考文献
Funabashi et al.
Bulletin of the Chemical Society of Japan, 1969 , vol. 42, p. 2885
反应条件
palladium dichloride in acetonitrile
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 33 p. 7670 - 7673
反应条件
1: palladium dichloride / acetonitrile 2: 10 palladium on activated charcoal; palladium dichloride / acetonitrile / 24 h / 80 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 33 p. 7670 - 7673
反应条件
hydrogenchloride; water
参考文献
Zhurnal Obshchei Khimii, , vol. 24, p. 131; engl. Ausg. S. 127
反应条件
1: palladium dichloride / acetonitrile 2: 10 palladium on activated charcoal; palladium dichloride / acetonitrile / 24 h / 80 °C View Scheme
参考文献
Matsubara, Yoshio; Hirakawa, Saori; Yamaguchi, Yoshihiro; Yoshida, Zen-Ichi
Angewandte Chemie - International Edition, 2011 , vol. 50, # 33 p. 7670 - 7673