4-甲氧基-2-苯基苯乙酮合成路线 (共 128 条)
反应条件
1: 51 percent
2: 65 percent / H2SO4, NaNO2
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参考文献
Joshi, Vidya; Jalisatgi, S. S.; Hari, M. I.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 83 - 84
反应条件
1: amalgamated zinc; aqueous HCl
2: methyl magnesium iodide; diethyl ether / Erhitzen des Rueckstands auf 180-200grad
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参考文献
Brownlee et al.
Biochemical Journal, 1943 , vol. 37, p. 572,575
反应条件
1: sodium ethylate; ethanol
2: ethanol; NH2OH+HCl
3: ethanolic sodium ethylate
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参考文献
Takagi; Yasuda
Yakugaku Zasshi, 1959 , vol. 79, p. 467,469
Chem.Abstr., 1959 , p. 18003
反应条件
sodium tetrahydroborate in ethanol
参考文献
Shankaran, K.; Rao, A.S.
Synthetic Communications, 1980 , vol. 10, # 7 p. 573 - 580
参考文献
Jenkins
Journal of the American Chemical Society, 1932 , vol. 54, p. 1155,1161
反应条件
1: bromine / CHCl3
2: 89 percent / DMSO / 4 h / 100 - 120 °C
3: 71 percent / 40 percent aq. NaOH / ethanol; H2O / 3 h / Heating
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参考文献
Schwenker; Guo
Archiv der Pharmazie, 1993 , vol. 326, # 1 p. 45 - 50
参考文献
Bruzau
Annales de Chimie (Cachan, France), 1934 , vol. <11> 1, p. 257,276
Full Text Show Details
Ramart-Lucas; Bruzau
Bulletin de la Societe Chimique de France, 1934 , vol. <5> 1, p. 119,136
反应条件
1: 97 percent / Zn; I2 / benzene / 1 h / Heating
2: 90 percent / Et3SiH; TFA; BF3*Et2O / CH2Cl2 / 8 h / Heating
3: 92 percent / aq. KOH / 8 h / Heating
4: 85 percent / polyphosphoric acid / 1 h / 80 °C
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参考文献
Jung, Jae-Chul; Lee, Ji-Ho; Oh, Seikwan; Lee, Jae-Gon; Park, Oee-Sook
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 22 p. 5527 - 5531