叔丁基二甲基硅氧烷基乙醛合成路线 （共 20 条）
反应条件
pyridine; oxalyl dichloride; dimethyl sulfoxide in dichloromethane T=-65°C;
参考文献
Belov, Vladimir N.; Korneev, Sergei M.; Angerer, Juergen; De Meijere, Armin
European Journal of Organic Chemistry, 2008 , # 26 p. 4417 - 4425
反应条件
sodium periodate; osmium(VIII) oxide in diethyl ether; water; tert-butyl alcohol T=23°C; 2 h;
参考文献
Sodeoka, Mikiko; Yamada, Hiroyoshi; Shibasaki, Masakatsu
Journal of the American Chemical Society, 1990 , vol. 112, # 12 p. 4906 - 4911
反应条件
1: With ozone in dichloromethane T=-78°C; 2: With triphenylphosphine in dichloromethane T=-78 - 20°C;
参考文献
Lafontaine, Jennifer A.; Provencal, David P.; Gardelli, Cristina; Leahy, James W.
Journal of Organic Chemistry, 2003 , vol. 68, # 11 p. 4215 - 4234
反应条件
1: With oxygen; ozone in dichloromethane T=-78°C; 2: With triphenylphosphine in dichloromethane T=-78 - 20°C; Inert atmosphere;
参考文献
Vanler, Sebastien F.; Larouche, Guillaume; Wurz, Ryan P.; Charette, Andre B.
Organic Letters, 2010 , vol. 12, # 4 p. 672 - 675
反应条件
1.1: Et3N; DMAP / tetrahydrofuran / 20 °C 2.1: O3 / methanol / -78 °C 2.2: NaHCO3; Me2S / methanol / -78 - 20 °C View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 6 p. 755 - 767
反应条件
1: With ozone in dichloromethane T=-78°C; 2: With 2,3-dimercapto-succinic acid in dichloromethane T=20°C;
参考文献
Synlett, , # 1 p. 33 - 36
反应条件
pyridine; hydrogenchloride; triethylamine in dichloromethane; dimethyl sulfoxide
反应条件
sodium periodate in dichloromethane; water Yield given;
参考文献
Synthetic Communications, , vol. 18, # 4 p. 359 - 366
反应条件
ozone in dichloromethane T=-78°C;
参考文献
Tetrahedron, , vol. 57, # 8 p. 1515 - 1524
