N-(2-氯苯基)-苯酰胺合成路线 (共 42 条)
反应条件
T=25°C; Geschwindigkeit;
参考文献
Orton; Bradfield
Journal of the Chemical Society, 1927 , p. 988,995
参考文献
Jadhav; Sukhtankar
Journal of the Indian Chemical Society, 1938 , vol. 15, p. 649,651
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Meybeck
Annales de Chimie (Cachan, France), 1932 , vol. <10>7, p. 129,198
参考文献
King; Orton
Journal of the Chemical Society, 1911 , vol. 99, p. 1378,1380
反应条件
sulfuric acid 3 h; Heating;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 22, # 9 p. 872 - 877
反应条件
1: Lawesson's reagent / xylene / 2.5 h / 105 - 115 °C 2: Cs2CO3 / xylene / 5 h / Heating View Scheme
参考文献
Synlett, , # 13 p. 2121 - 2123
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate in ethylene glycol dimethyl ether 48 h; Heating;
参考文献
Evindar, Ghotas; Batey, Robert A.
Journal of Organic Chemistry, 2006 , vol. 71, # 5 p. 1802 - 1808
反应条件
palladium diacetate; sodium carbonate in N,N-dimethyl acetamide T=100 - 170°C; 36 h;
参考文献
Ames, D.E.; Opalko, A.
Tetrahedron, 1984 , vol. 40, # 10 p. 1919 - 1926
反应条件
1: phosphorus pentachloride / dichloromethane / 24 h / |Inert atmosphere; |Reflux
2: sodium t-butanolate; palladium diacetate; N-[2'-(dicyclohexylphosphino)-1,1'-biphenyl-2-yl]-N,N-dimethylamine / toluene / 18 h / 100 °C / |Inert atmosphere
View Scheme
参考文献
Sadig, Jessie E. R.; Foster, Radleigh; Willis, Michael C.; Wakenhut, Florian
Journal of Organic Chemistry, 2012 , vol. 77, # 21 p. 9473 - 9486,14
参考文献
Grimshaw, James; Silva, A. Prasanna de
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 857 - 866
反应条件
zinc(II) chloride
anschliessendes Erhitzen mit wss. H2SO4;
参考文献
Dippy; Moss
Journal of the Chemical Society, 1952 , p. 2205,2207, 2209